Analysis of Diethanolamide Reaction by using FTIR Technique

Authors

  • Sandeep B. Mundhe Department of Chemical Engineering, Jawaharlal Nehru Engineering College, Dr. Babasaheb Ambedkar Marathvada University, Aurangabad, Maharashtra, India
  • Sonali D. Anbhule Department of Chemical Engineering, Jawaharlal Nehru Engineering College, Dr. Babasaheb Ambedkar Marathvada University, Aurangabad, Maharashtra, India

DOI:

https://doi.org/10.37591/jocc.v3i1.2241

Abstract

The purpose of this work is to study the amidification reaction for production of diethanolamide from ethyl acetate and diethanolamine by using sulfuric acid catalyst. The amidation, which is the reaction between ethyl acetate and diethanolamine, was held in a glass batch reactor with mole ratio 1:1 using acid catalyst (H2SO4) 0.5% (w/w) and 200 rpm stirring. The reaction temperature is 160°C constant, and sampling was performed after every 30 min. The analysis includes Fourier transfer infra-red (FT-IR) to know the structure of amide.

 

Keywords: Amidation, diethanolamine, diethanolamide, ethyl ester, temperature, reaction rate

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Published

2019-04-15

Issue

Vol. 3 No. 1 (2016)

Section

Articles

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